The effect of reaction temperature change on equilibrium 52287-51-1

As far as I know, this compound(52287-51-1)Quality Control of 6-Bromo-2,3-dihydrobenzo[b][1,4]dioxine can be applied in many ways, which is helpful for the development of experiments. Therefore many people are doing relevant researches.

In general, if the atoms that make up the ring contain heteroatoms, such rings become heterocycles, and organic compounds containing heterocycles are called heterocyclic compounds. An article called Novel synthesis of p-benzoquinone ethylene acetal, published in 1975, which mentions a compound: 52287-51-1, Name is 6-Bromo-2,3-dihydrobenzo[b][1,4]dioxine, Molecular C8H7BrO2, Quality Control of 6-Bromo-2,3-dihydrobenzo[b][1,4]dioxine.

PhO(CH2)2OH (I) reacted with HgO-iodine reagent (II) in the dark to give 4-RC6H4O(CH2)2OH (III; R = I). Irradiation of III (R = I) in the presence of II gave 84% title compound (IV). In contrast, irradiation of I directly, in the presence of II, gave in addition to 34% IV, 31% III (R = I), 9-14% benzodioxins V (R = H, I), and 6% p-benzoquinone. NMR studies showed that III (R = Br, Cl) were stable to II in the dark but on irradiation gave 16% IV and 30-5% V (R = Br, Cl, resp.). The mechanism for the formation of IV involved formation of an alkoxyl radical followed by cyclization and halo-elimination.

As far as I know, this compound(52287-51-1)Quality Control of 6-Bromo-2,3-dihydrobenzo[b][1,4]dioxine can be applied in many ways, which is helpful for the development of experiments. Therefore many people are doing relevant researches.

Reference:
Pyrazole – Wikipedia,
Pyrazoles – an overview | ScienceDirect Topics