In the chemical reaction process, reaction time, type of solvent, can easily affect the result of the reaction, thereby determining the yield and properties of the reaction product. An updated downstream synthesis route of 75415-03-1 as follows. Safety of 2-(1H-Pyrazol-3-yl)pyridine
A mixture of HL (0.2 mmol, 29 mg), Zn(NO3)26H2O (0.2 mmol, 59 mg),ethanol (1 ml), and H2O (10 ml) was stirred for 0.5 h in air, then the resulting mixture was transferred in a Teflon-linedstainless reactor and heated to 140 C for 3 days under autogenous pressure and cooled to room temperature at a rate of10 C/h. Consequently, the colorless block-shaped crystals suitable for X-ray single crystal diffraction were obtained witha yield of 36.7 % (based on Zn(NO3)26H2O)
According to the analysis of related databases, 75415-03-1, the application of this compound in the production field has become more and more popular.
Reference:
Article; Liu; Huan; Cui; Han; Journal of Structural Chemistry; vol. 56; 6; (2015); p. 1124 – 1129; Zh. Strukt. Kim.; vol. 56; 6; (2015); p. 1177 – 1182,6;,
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