The origin of a common compound about 1-(Tetrahydro-2H-pyran-4-yl)-1H-pyrazol-4-amine

According to the analysis of related databases, 1190380-49-4, the application of this compound in the production field has become more and more popular.

Each compound has different characteristics, and only by selecting the characteristics of the compound suitable for a specific situation can the compound be applied on a large scale. 1190380-49-4, name is 1-(Tetrahydro-2H-pyran-4-yl)-1H-pyrazol-4-amine, This compound has unique chemical properties. The synthetic route is as follows., Recommanded Product: 1-(Tetrahydro-2H-pyran-4-yl)-1H-pyrazol-4-amine

General procedure: [00495] A mixture of 2-chloro-N-(( 1 r,4r)-4-morpholinocyclohexyl)-5 -phenyl-7-tosyl-7H-pyrrolo [2,3 – djpyrimidin-4-amine (79 mg, 0.14 mmol, 1.0 eq), 1-(tetrahydro-2H-pyran-4-yl)-1H-pyrazol-4-amine 9 (49mg, 0.30 mmol, 2.3 eq), and trifluoroacetic acid (0.20 mL, 2.6 mmol, 19 eq) in 2.0 mL of isopropanol was heated at 120 C in a capped vial for 4 hr. The reaction mixture was cooled to room temperature and purified on reverse phase HPLC giving N4-(( 1 r,4r)-4-morpholinocyclohexyl)-5 -phenyl-N2-( 1 -(tetrahydro-2H-pyran- 4-yl)-1H-pyrazol-4-yl)-7H-pyrrolo[2,3-djpyrimidine-2,4-diamine as a white powder after lyophilization (1.9 mg, 2% yield). LC-MS: M+H=543.3. Also isolated 30 mg of beige solid as N4-((lr,4r)-4- morpholinocyclohexyl)-5 -phenyl-N2-(1 -(tetrahydro-2H-pyran-4-yl)- 1H-pyrazol-4-yl)-7-tosyl-7H- pyrrolo [2,3 -djpyrimidine-2,4-diamine (31% yield).

According to the analysis of related databases, 1190380-49-4, the application of this compound in the production field has become more and more popular.