Adding a certain compound to certain chemical reactions, such as: 3469-69-0, name is 4-Iodopyrazole, belongs to pyrazoles-derivatives compound, can increase the reaction rate and produce products with better performance than those obtained under traditional synthetic methods. Here is a downstream synthesis route of the compound 3469-69-0, Recommanded Product: 3469-69-0
Diisopropylethylamine (DIEA, 1.75 ml, 10 mmol) and trimethylsilylethoxymethyl chloride (SEMCl, 1.83 ml, 10 mmol) are added, under argon, to a solution of 4-iodopyrazole (1.94 g, 10 mmol) in CH2Cl2 (100 ml). The mixture is stirred overnight at ambient temperature. The solvent is evaporated off under vacuum. The residue is taken up with a diethyl ether/water mixture. The organic phase, after drying and evaporation, gives a colourless oil which is purified by elution on silica gel with an EtOAc/CH2Cl2 (5/95) mixture. 3.02 g of product are obtained in the form of a colourless oil.
In the field of chemistry, the synthetic routes of compounds are constantly being developed and updated. I will also mention this compound in other articles, 4-Iodopyrazole, other downstream synthetic routes, hurry up and to see.